Methods of Analytical Measurement

Course guarantor:

Hana Průšová

Lecturer:

Hana Průšová

Tutor:

Hana Průšová

Supervisor:

Department of Dosimetry and Application of Ionizing Radiation

Synopsis:

Principles, technical performance and utilization of methods of chemical analysis. Methodology of analytical determination, gravimetry, titration methods, potentiometry, polarography, refractometry, polarimetry, UV-VIS spectroscopy, atomic emission and absorption spectroscopy, infrared and Raman spectroscopy, X-ray structural analysis, nuclear magnetic and electron spin resonance, mass spectrometry, thermometric methods, gas and liquid chromatography.

Requirements:

Syllabus of lectures:

1. Principle, realisation and use of chemical analytical methods. Methodology of determination.

2. Classic methods: Gravimetry, titration methods.

3. Electrochemical methods: potenciometry, polarography, voltametry, coulometry.

4. Optical methods.

5. Atomic emission and absorption spektroscopy.

6. Roentgen structural analysis, nuclear magnetic and electron spin resonance.

7. Mass spectrometry.

8. Thermometric methods,entalpiometry, thermogravimetry, differential thermal analysis.

9. Separation methods: extraction, gas and liquid chromatography, paper chromatography.

10. Method comparison.

11. New trends in analytical chemistry.

Syllabus of tutorials:

Study Objective:

Knowledge:

Orientation in principles of methods of physical and chemical analysis of matter.

Abilities:

The orientation of the individual methods of analysis of a meaningful use in practical cases.

Study materials:

Key references:

[1] John Kenkel: Analytical Chemistry for Technicians, CRC Press, Boca Raton 2014

Recommended references:

[2] Douglas A. Skoog: Analytical Chemistry: An Introdution, Saunders College Pub., 2000

[3] Peter Atkins, Julio de Paula: Fyzikální chemie, VŠCHT v Praze, 2013

Note:

Time-table for winter semester 2024/2025:

Time-table is not available yet

Time-table for summer semester 2024/2025:

Time-table is not available yet

The course is a part of the following study plans:

• Jaderné inženýrství - Aplikovaná fyzika ionizujícího záření (PS)
• Radiolgická fyzika (elective course)
• Vyřazování jaderných zařízení z provozu (elective course)