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CZECH TECHNICAL UNIVERSITY IN PRAGUE
STUDY PLANS
2023/2024
UPOZORNĚNÍ: Jsou dostupné studijní plány pro následující akademický rok.

Structure Analysis 2

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Code Completion Credits Range
15NMR Z,ZK 3 2P+1C
Garant předmětu:
Lecturer:
Tutor:
Supervisor:
Department of Nuclear Chemistry
Synopsis:
Requirements:

Individual work of students based on interpretation spectral data examples of simple NMR spectra. Results will be evaluated by examination.

Syllabus of lectures:

1. Principles of nuclear magnetic resonance. Magnetic properties of nuclei, resonance signal genesis, nuclear shielding and chemical shift, spin-spin interaction, relaxation mechanisms, NMR signal intensities.

2. NMR spectrometer - Basic components, types of construction, measurement techniques. Fourier transform Double resonance. Measurement of relaxation times. Solvent signal suppression.

3.Sample preparation, solvents, standards.

4. 1H-NMR techniques.

5. 13C-NMR techniques.

6. 15N, 18F, 31P, 2H, 3H and other measurement techniques.

7. Special NMR techniques. 2D-NMR (COSY, NOESY, TOCSY, HETCOR), solid-state NMR (MAS).

8. Interpretation of spectral data: 1H, 13C, 15N, 31P, special techniques 3H/2H

9. Interpretation and measurements of APT, DEPT, COESY, NOESY, TOCSY, HQMBC isotopic composition manifestations

10. Application of NMR.

Syllabus of tutorials:
Study Objective:

Acquired knowledge:

Students learn about generation of NMR signal, magnetic parameters of nuclei, spin-spin interaction, interpretation of spectral data in NMR.

Acquired skills:

The emphasis is put on correct evaluation of NMR spectra and identification of compounds.

Study materials:

Key Literature:

1.Gunther H.: NMR Spectroscopy: Basic Principles, Concepts and Applications in Chemistry. Willey 2013.

Recommended Literature:

1.Williams D.H., Fleming I.: Spectroscopic methods in organic chemistry. 5th eddition.

Note:
Time-table for winter semester 2023/2024:
Time-table is not available yet
Time-table for summer semester 2023/2024:
Time-table is not available yet
The course is a part of the following study plans:
Data valid to 2024-04-15
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