Experimental Methods of Study Material

Garant předmětu:

Lecturer:

Tutor:

Supervisor:

Department of Materials Engineering

Synopsis:

Methods of diffraction: X-ray and electron diffraction (for the phase analysis to determine the residual stress, texture, and for analysis of lattice defects). Display methods: light and electron microscopy (preparation of sample and display characteristics, preparation of contrast theory). Advanced Methods of physical and chemical microanalysis: scanning electron microscopy (emission, transmission and conductivity method). Electron probe microanalysis: wavelength and energy dispersive X-ray spectroscopy, quantitative microanalysis, signal processing.

Requirements:

Syllabus of lectures:

1.Light microscopy (sample preparation and display characteristics, contrast theory)

2.Confocal microscopy, light spectroscopy methods analysis (GDOES, etc.)

3.The electrons, interact with the sample I, transmission electron microscopy (principle, sample preparation)

4.Transmission electron microscopy (display characteristics, contrast theory)

5.Special methods of TEM (HV TEM, HR TEM)

6.Scanning electron microscopy (principle, sample preparation)

7.Scanning electron microscopy (display characteristics, contrast theory)

8.Electron diffraction (phase analysis, residual stress, texture, lattice defects)

9.The interaction of electrons with the sample, x-ray spectroscopy, the analysis of the chemical composition, EDS and WDS, XRS

10.Methods SPM

11.Quantitative X-ray microanalysis

12.Electron and ion spectroscopy

13.Electron and ion spectroscopy and microanalysis

Syllabus of tutorials:

Study Objective:

Study materials:

Note:

Further information:

No time-table has been prepared for this course

The course is a part of the following study plans: