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CZECH TECHNICAL UNIVERSITY IN PRAGUE
STUDY PLANS
2025/2026

Analytical Electron Microscopy

The course is not on the list Without time-table
Code Completion Credits Range
D14AEM ZK 2P
Course guarantor:
Lecturer:
Tutor:
Supervisor:
Department of Materials
Synopsis:

Inelastic scattering processes with energy losses are often element-specific and so they are used for chemical analysis in the transmission electron microscope. The course deals with the theory of the electron scattering, electron energy loss spectroscopy,energy dispersive X-ray spectroscopy and cathodoluminiscence.

Requirements:
Syllabus of lectures:

1. Introduction to analytical methods

2. Elastic scattering of electrons - Rutherford scattering, scattering on shielded potential, Bragg scattering, scattering on phonons

3. Inelastic scattering of electrons - Bethe theory, dielectric formalism, plasmon excitations, differential cross-section, Kramers-Kronig analysis, multiple scattering, ionization edges, energy loss near edge structure (ELNES)

4. Electron energy loss spectroscopy (EELS) spectrometer, energy resolution, detection of electron losses, spatial resolution

5. Energy filtered TEM zero loss filtering, plasmon filtering, elemental mapping

6. Energy dispersive spectroscopy of characteristic X-rays (EDX) - spectrometer, interaction volumes, artefacts

7. Cathodoluminiscence - description of the spectrometer, diffraction on a slit, diffraction on a grid, pair electron-hole recombination, Cerenkov radiation, transition radiation

8. Chemical microanalysis (EELS, EDX)

9. Current research topics - plasmonics, phase manipulation, imaging of atomic orbitals

Syllabus of tutorials:
Study Objective:
Study materials:

[1] R.F. Egerton, Electron Energy-Loss Spectroscopy in the Electron Microscope, 3rd ed., Springer, Berlin, 2011.

[2] R. Brydson, Electron Energy Loss Spectroscopy, Taylor and Francis, London, 2001.

[3]C. C. Ahn, Transmission Electron Energy Loss Spectrometry in Materials Science and the EELS ATLAS, 2nd ed., Wiley-VCH, Weinheim, 2004.

Note:
Further information:
No time-table has been prepared for this course
The course is a part of the following study plans:
Data valid to 2025-03-31
For updated information see http://bilakniha.cvut.cz/en/predmet6582506.html