Methods of Analytical Measurement

Lecturer:

Václav Spěváček (gar.)

Tutor:

Václav Spěváček (gar.)

Supervisor:

Department of Dosimetry and Application of Ionizing Radiation

Synopsis:

Principles, technical performance and utilization of methods of chemical analysis. Methodology of analytical determination, gravimetry, titration methods, potentiometry, polarography, refractometry, polarimetry, UV-VIS spectroscopy, atomic emission and absorption spectroscopy, infrared and Raman spectroscopy, X-ray structural analysis, nuclear magnetic and electron spin resonance, mass spectrometry, thermometric methods, gas and liquid chromatography, analytical data processing, chemometry

Requirements:

01MAST

Syllabus of lectures:

1.Principle, realisation and use of chemical analytical methods. Methodology of determination.

2.Classic methods: Gravimetry, titration methods.

3.Electrochemical methods: potenciometry, polarography, voltametry, coulometry.

4. Refractometry, polarimetry.

5. Lambert-Beer law, coulorimetry, UV-VIS spectroscopy.

6. Atomic emission and absorption spektroscopy.

7. Vibrational spectra, IR and Raman spectroscopy.

8. Roentgen structural analysis, nuclear magnetic and electron spin resonance.

9. Mass spectrometry.

10. Thermometric methods,entalpiometry, thermogravimetry, differential thermal analysis.

11. Separation methods: extraction, gas and liquid chromatography, paper chromatography.

12.Treatment of analytical results, chemometrics.

Syllabus of tutorials:

Study Objective:

Knowledge:

Orientation in principles of methods of physical and chemical analysis of matter.

Abilities:

The orientation of the individual methods of analysis of a meaningful use in practical cases.

Study materials:

Key references:

[1]Josef Zika (at al.): Analytical guide, SNTL Prague 1966(and later edition)(in Czech)

[2]Pavel Klouda: Modern analytical methods,P.Klouda Ostrava 1996(in Czech)

Recommended references:

[3]Milan Meloun, Jiri Militky: Statistical processing of experimental data,

Plus Prague 1994(in Czech)

Note:

Time-table for winter semester 2011/2012:

Time-table is not available yet

Time-table for summer semester 2011/2012:

Time-table is not available yet

The course is a part of the following study plans: